CaMKII-IN-1_LCMS_13615_MedChemExpress

File ..720 2017-07-20 08-37-36\CPK2017-720-13615.D Tgt Mass (CHM): Injection Date : 20 Jul 17 3:06 pm +0800 Seq. Line : 79 Sample Name : CPK2017-720-13615 Location : P1-B-08 Acq. Operator : ZLJ_587 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul

Acq. Method : D:\chem32\1\DATA\20170720\20170720 2017-07-20 08-37-36\1-POS-3MIN.M Analysis Method : D:\CHEM32\1\DATA\20170720\20170720 2017-07-20 08-37-36\1-POS-3MIN.M Catalog No : HY-18271 Batch#13615 A-RP-186

Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min

Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C

min

0.5

1 1.5

2 2.5mAU 0

200400600 DAD1 B, Sig=214,4 Ref=off

0.539

1.521

1.580

1.796

min

0.51

1.5

2 2.5mAU 0

100

200

DAD1 C, Sig=254,4 Ref=off 1.521

1.582

1.798

min

0.51

1.52

2.50

20000

4000060000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70

1.552

min

0.5

1

1.52

2.5-0.1

-0.0500.05 Ion 1, MSD1 1,Target Mass 0 +H Positive, EIC=0.7:1.7 Integration Results for DAD1 B, Sig=214,4 Ref=off

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.54 0.02 6.87 5.22 0.37 ND 1.52 0.03 1808.19 920.86 98.09 548 1.58 0.02 25.49 20.10 1.38 548 1.80 0.02 2.77 2.67 0.15 ND

Integration Results for DAD1 C, Sig=254,4 Ref=off

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.52 0.03 687.56 351.14 98.62 548 1.58 0.02 7.67 6.59 1.10 548 1.80 0.02 1.99 1.36 0.28 ND

Integration Results for MSD1 TIC, MS File

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.55 0.05 212057.16 74769.86 100.00 548

Ret. Time: 1.55 <<<< POSITIVE SPECTRA >>>>

m/z

200

300

400

500

600

700

800

1000

20003000

40005000

600070008000 ES-API Positive

460.0

275.5

551.1 549.2

548.2