Cefozopran_hydrochloride_LCMS_13992_MedChemExpress

=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 18Acq. Instrument : HY-LCMS-02 Location : Vial 16Injection Date : 11/27/2014 10:32:04 AM Inj : 1 Inj Volume : 3.000 μl Acq. Method : D:\AGLIENT 1260\DATA\20141127\20141127 2014-11-27 09-03-48\100-1000MS+3MIN( 0.02%FA).M Last changed : 11/27/2014 9:04:36 AM by Kang Li(LCMS-02)Analysis Method : D:\AGLIENT 1260\DATA\20141202\20141202 2014-12-02 09-27-53\20-25A-80A,280.M (Sequence Method)Last changed : 12/3/2014 9:44:17 AM by Li Shan(LCMS-02) (modified after loading)Method Info : hplc A-RP-32 Additional Info : Peak(s) manually integrated min

0.51 1.52 2.53mAU -200

-100

0100200300400 DAD1 B, Sig=214,4 Ref=off (D:\AGLIENT...60\DATA\20141127\20141127 2014-11-27 09-03-48\BIZ2014-N27-DJL1.D)

A r e a : 104.733 0.396 A r e a : 2077.21

0.442 ===================================================================== Area Percent Report ===================================================================== Sorted By : Signal Multiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 B, Sig=214,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 0.396 MF 0.0331 104.73349 52.79257 4.8000 2 0.442 FM 0.0490 2077.20874 706.28076 95.2000 Totals : 2181.94223 759.07333 ===================================================================== *** End of Report ***

Catalog No : HY-B0771A Batch#13992

=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 18Acq. Instrument : HY-LCMS-02 Location : Vial 16Injection Date : 11/27/2014 10:32:04 AM Inj : 1 Inj Volume : 3.000 μl Acq. Method : D:\AGLIENT 1260\DATA\20141127\20141127 2014-11-27 09-03-48\100-1000MS+3MIN( 0.02%FA).M Last changed : 11/27/2014 9:04:36 AM by Kang Li(LCMS-02)Analysis Method : D:\AGLIENT 1260\DATA\20141126-1\20141126-1 2014-11-26 17-14-00\100-1000MS+ 3MIN.M (Sequence Method)Last changed : 11/27/2014 11:24:29 AM by Li Shan(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-102,40℃ Catalog No : HY-B0771A Batch#13992 A-RP-32 Additional Info : Peak(s) manually integrated min

0.51 1.52 2.530

50000

100000

150000

200000

250000

300000

MSD1 TIC, MS File (D:\AGLIENT 1260\DATA\20141127\20141127 2014-11-27 09-03-48\BIZ2014-N27-DJL1.D) ES-API, Pos, Sca

0.447

MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. Weight Time (MS) MS Area or Ion 0.447 1399029 518.00 I 517.00 I 516.00 I 258.50 I 120.00 I

m/z

200400600800020

40

60

80

100

*MSD1 SPC, time=0.432:0.469 of D:\AGLIENT 1260\DATA\20141127\20141127 2014-11-27 09-03-48\BIZ2014-N27-DJL1.D ES-API,Max: 100504 518.0

120.0 258.5 516.0 *** End of Report ***