Sample for review 外文杂志审稿样本

Molecules (ISSN 1420-3049) Referee Report Form

https://www.wendangku.net/doc/2517937206.html,/molecules/

Manuscript ID: molecules-20071212-Soomro-be

Type of the paper: Full Paper

Title: Synthesis and Photochemistry of Polyene Cored Stilbenoid Dendrimer

Authors: Shahid A. Soomro 1,* and Saeeda Aziz-Soomro 2

E-mail: shahid.soomro@dafra.be

Received: 11 December 2007

Manuscript file:

https://www.wendangku.net/doc/2517937206.html,/molecules/temp/molecules-20071212-Soomro-be.doc

(size 104 KB)

1. OVERALL EVALUATION

2. OVERAL L RECOMMENDATION:

3. Comments and Suggestions (for author to read)

The manuscript “Synthesis and Photochemistry of Polyene Cored Stilbenoid Dendrimer” from Soomro et al. describes the synthesis of first generation dendrimer; a polyene core decorated with four stilbene chromophores. The photophysical study is presented.

I cannot recommend the manuscript for publication in the present form; however, after major revision it could be considered again.

1) Introduction

First the introduction is not clear. From the rest of the manuscript it becomes evident that authors direct their interest to light harvesting; however; in the introduction references are missing related to light harvesting dendrimers, e.g. by Müllen et al. and Moore et al. . Moreover, a reference regarding stilbenoid dendrimers, energy and electron transfer is also missing: H. Meier, M. Lehmann "STILBENOID DENDRIMERS - PREPARATION AND PROPERTIES " in H.S. Nalwa (Ed.), Encyclopedia of Nanoscience and Nanotechnology, Vol. 10, 95-106, American Scientific Publishers, Stevensons Ranch 2004.

Page 2: a) The new structural concept was envisioned from H. Meiers Group (Angewandte Chemie 1998) almost parallel to the group of Prof. Luping Yu (JACS 1997).

b) Since the authors, which performed obviously some work under supervision of Prof. H. Meier (see reference 3, 6 and the PhD thesis Mainz 2005; http://ubm.opus.hbz-nrw.de/frontdoor.php?source_opus=754); wrote “we envisioned”, I suppose that t hey meant their research group. However, nobody from the former authors (Angew. Chem. Int. Ed.1998, 37, 643-645) can be found among the authors. Thus, either the authors need to write “The structural concept was envisioned + references….” or they include simply one of the former authors. Furthermore, it remains unclear how the presented dendrimers are tunable with respect to page 2 of the introduction and what the authors mean by “two fold dendrimers”.

A very similar publication where the conjugation between periphery and polyen core is broken by meta-substitution is cited as reference 12. However, the idea presented here, is already given in the later paper. The difference between reference 12 and the presented molecules should be already discussed in the introduction.

2) Results and discussion – synthesis

Page 3, the twofold Williamson’s ether synthesis leads to the product 5. It is quite normal that a slight excess of bromide 3 is used; however, the reaction is no bromination but an alkylation of a phenolic OH group!

PCC should be explained in the text.

I wonder if the chromatographic separation was really done on a SiO2 column. The solid phase is usually silica which has not the composition SiO2, which is quartz.

The authors probably wanted to wr ite “with almost all-trans configuration”. Frequently, the Horner reaction gives less than 10 % Z configured stilbene. I would recommend to show an NMR spectrum where the integration shows the composition of the product. Moreover, authors should not use cis and trans, but E and Z.

3) Results and discussion – UV/Vis and fluorescence

It is well known, that interaction of transition dipoles leads to a so called F?rster transfer of energy. It is certainly not a simple dipole-dipole interaction as described by the authors. This chapter should be completely revised.

If the authors describe the excitation of different chromophores, they should give also the spectral band width of their light source.

The fluorescence data is ill-interpreted. On the basis of Figure 1 and 2 the emission comes almost exclusively from the core. However, authors should show absorption and fluorescence data in one diagram also including the fluorescence below 400 nm.

It is certainly not true that the only the peaks at 536, 552 are related with the core emission. The intensity of the emission spectra is in line with an exclusive core emission and light harvesting process; this part should be completely rewritten.

Moreover, authors state that the core can not be separately excited! It is just the opposite!! The peripheral stilbene units can not selectively excited, however, the core can be excited selectively at the absorption edge at long wavelengths. I suppose that this is the reason that the emission is lowest when the chromophore is excited at 385 nm, compared to the irradiation at 314 nm.

Finally, stilbenes and polyenes are each conjugated, i.e. they “have pi-conjugation” however, there is no conjugation between them!!

4) Experimental

Synthesis of 2 and 3 is known from literature and there is no need for their description unless there is a change of the procedure.

There are many formal and spelling errors, e.g. numbers in formula need to be written as subscripts etc. and for the procedure of compound 5 it should be written phenyl ins tead of “phenly”; the amount of compounds should be given with uniform number of digits; etc.

The elemental analysis for compounds 5 and 8 are wrong and are given without any comment!! Either they should be repeated or the reason for such a big deviation has to be explained. Certainly SiO2 should be silica.

4. Comments (for editor)

This manuscript describes the synthesis and characterization of a series of new diketopyrrolopyrrole-based luminophores and their photoluminescence properties as well in solution as in solid state. Absorption and emission characteristics were extensively analyzed and conclusions were drawn considering the molecular design in solution and in solid state. Also the single crystal structures of some of the DPP-compounds were elucidated and the structure-property relationships were consequently established. Therefore this manuscript meets the requirements for publishing in this journal. However, This paper requires very substantial / major revisions to both technical content and language. I suggest technical issues are dealt with first and then the language is polished after a second review.

主题: 审稿

各位同学: 你们好！

请对文章是否新颖并有实质性的内容，实验设计是否合理，图表是否合理，英文是否通顺，结论是否合理等予以综合评价，并对发表前需作哪些修改和补充，提出具体意见，审稿意见请于10天内返回。谢谢！

如果发现相同或者很相似的文献，证明该文章没有什么创新性，请把文献附上。

英语的修改可以在稿件上直接进行。

有一份附件是审稿的样板。供参考。

曹德榕

一些英文审稿意见及回复的模板

最近在审一篇英文稿，第一次做这个工作，还有点不知如何表达。幸亏遇上我的处女审稿，我想不会枪毙它的，给他一个major revision后接收吧。呵呵 网上找来一些零碎的资料参考参考。 +++++++++++++++++++++++++++++++ 1、目标和结果不清晰。 It is noted that your manuscript needs careful editing by someone with expertise in technical English editing paying particular attention to English grammar, spelling, and sentence structure so that the goals and results of the study are clear to the reader. 2、未解释研究方法或解释不充分。 In general, there is a lack of explanation of replicates and statistical methods used in the study. Furthermore, an explanation of why the authors did these various experiments should be provided. 3、对于研究设计的rationale: Also, there are few explanations of the rationale for the study design. 4、夸张地陈述结论/夸大成果/不严谨： The conclusions are overstated. For example, the study did not show if the side effects from initial copper burst can be avoid with the polymer formulation.

一些英文审稿意见的模板【转】

一些英文审稿意见的模板【转】最近在审一篇英文稿第一次做这个工作还有点不知如何表达。幸亏遇上我的处女审稿我想不会枪毙它的给他一个major revision后接收吧。呵呵网上找来一些零碎的资料参考参考。1、目标和结果不清晰。It is noted that your manuscript needs careful editing by someone with expertise in technical English editing paying particular attention to English grammar spelling and sentence structure so that the goals and results of the study are clear to the reader. 2、未解释研究方法或解释不充分。In general there is a lack of explanation of replicates and statistical methods used in the study. Furthermore an explanation of why the authors did these various experiments should be provided. 3、对于研究设计的rationale: Also there are few explanations of the rationale for the study design. 4、夸张地陈述结论/夸大成果/不严谨The conclusions are overstated. For example the study did not show if the side effects from initial copper burst can be avoid with the polymer formulation. 5、对hypothesis的清晰界定A hypothesis needs to be presented。6、对某个概念或工具使用的rationale/定义概念What was the rationale for the film/SBF volume ratio 7、对研究问题的定义Try to set the problem discussed in this paper in more clear write one section to define the problem 8、如何凸现原创性以及如何充分地写literature review: The topic is novel but the application proposed is not so novel. 9、对claim如AB的证明verification: There is no experimental comparison of the algorithm with previously known work so it is impossible to judge whether the algorithm is an improvement on previous work. 10、严谨度问题MNQ is easier than the primitive PNQS how to prove that. 11、格式重视程度In addition the list of references is not in our style. It is close but not completely correct. I have attached a pdf file with Instructions for Authors which shows examples. Before submitting a revision be sure that your material is properly prepared and formatted. If you are unsure please consult the formatting nstructions to authors that are given under the Instructions and Forms button in he upper right-hand corner of the screen. 12、语言问题出现最多的问题有关语言的审稿人意见It is noted that your manuscript needs careful editing by someone with expertise in technical English editing paying particular attention to English grammar spelling and sentence structure so that the goals and results of the study are clear to the reader. The authors must have their work reviewed by a proper translation/reviewing service before submission only then can a proper review be performed. Most sentences contain grammatical and/or spelling mistakes or are not complete sentences. As presented the writing is not acceptable for the journal. There are problems with sentence structure verb tense and clause construction. The English of your manuscript must be improved before resubmission. We strongly suggest that you obtain assistance from a colleague who is well-versed in English or whose native language is English. Please have someone competent in the English language and the subject matter of your paper go over the paper and correct it the quality of English needs improving. 作为审稿人本不应该把编辑部的这些信息公开冒风险啊但我觉得有些意见值得广大投稿人注意就贴出来吧当然有关审稿人的名字Email文章题名信息等就都删除了以免造成不必要的麻烦希望朋友们多评价其他有经验的审稿人能常来指点大家国人一篇文章投Mater.类知名国际杂志被塞尔维亚一审稿人打25分个人认为文章还是有一些创新的所以作为

材料类期刊投稿指南

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外文期刊名缩写规则与外文期刊缩写与全称对照表

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英文期刊审稿意见模板

1、目标和结果不清晰。 It is noted that your manuscript needs careful editing by someone with expertise in technical English editing paying particular attention to English grammar, spelling, and sentence structure so that the goals and results of the study are clear to the reader. 2、未解释研究方法或解释不充分。 In general, there is a lack of explanation of replicates and statistical methods used in the study. Furthermore, an explanation of why the authors did these various experiments should be provided. 3、对于研究设计的rationale: Also, there are few explanations of the rationale for the study design. 4、夸张地陈述结论/夸大成果/不严谨： The conclusions are overstated. For example, the study did not show if the side effects from initial copper burst can be avoid with the polymer formulation. 5、对hypothesis的清晰界定： A hypothesis needs to be presented。 6、对某个概念或工具使用的rationale/定义概念： What was the rationale for the film/SBF volume ratio? 7、对研究问题的定义： Try to set the problem discussed in this paper in more clear, write one section to define the problem 8、如何凸现原创性以及如何充分地写literature review: The topic is novel but the application proposed is not so novel. 9、对claim,如A＞B的证明，verification: There is no experimental comparison of the algorithm with previously known work, so it is impossible to judge whether the algorithm is an improvement on previous work. 10、严谨度问题： MNQ is easier than the primitive PNQS, how to prove that. 11、格式（重视程度）： In addition, the list of references is not in our style. It is close but not completely correct. I have attached a pdf file with "Instructions for Authors" which shows examples. Before submitting a revision be sure that your material is properly prepared and formatted. If you are unsure, please consult the formatting nstructions to authors that are given under the "Instructions and Forms" button in he upper right-hand corner of the screen. 12、语言问题（出现最多的问题）：

速度快并且容易中的材料类sci期刊

速度快并且容易中的材料类SCI期刊(更新中) 推荐： 1. Journal of alloy and compounds 影响因子IF 1点多，1个月给消息，容易中，现在几乎成为中国人的专刊了，哈哈； 2. applied surface science 影响因子IF 1点多，发表容易， 3. Materials Letter 1.7 速度快，快报一般都要求有新意（当然，新意太高可以投APL了） 4. Materials & Design 影响因子不到1，很快，快点一个月就接受的！适合特别想要文章毕业或者评奖学金的。 5. Physica B 影响因子不到1，很快，我一个同学已经在上面发了2篇了，最快不到一个月就接受了，还是容易中的，最好是工作全面细致些。 6. Materials science and engineering B 影响因子1点多，从投稿到接受一般3-4个月，相对容易中。 7. Optoelectronics and Advanced Materials-Rapid Communications, 罗马尼亚期刊，影响因子0.2，很快，一个月可以搞定，适合灌水和急需文章。 8. Optical materials 发光材料期刊，影响因子1点多，相对容易中，速度也快。 9. Journal of Luminescence 发光方面专业期刊，老牌杂志，虽然影响因子只有1点多，但很多发光方面的经典文章出自此期刊，相对容易中，速度也可以。 10. Journal of Physics D: Applied physics 偏物理材料方面，影响因子2 左右，速度快，也不难中，中国人投稿还比较多。 黑名单： 1. Thin solid films 影响因子1点多，但审稿巨慢，不推荐； 2. Materials Characterization 影响因子不高，容易中，但速度慢，如果不急着要文章，也可以投的； 3. Materials Chemistry and Physics 影响因子1点多，速度巨慢，我一个同学投稿半年还没消息，现在1年过去了还没查到这篇文章，估计没戏了吧。 4. Journal of Physics and Chemistry of Solids, 影响因子1点多，速度较慢，接受难度较易。

英文论文审稿意见范文

This paper addresses an important and interesting problem -automatically identifying adult accounts on Sina Weibo. The authors propose two sets of behavior indicators for adult groups and accounts, and find that adult groups and accounts have different behavioral distributions with non-adult groups and accounts. Then a novel relation-based model, which considers the inter-relationships among groups, individual accounts and message sources, is applied to identify adult accounts. The experimental results show that compared with state-of-the-art methods, the proposed method can improve the performance of adult account identification on Sina Weibo. Overall, the article is well organized and its presentation is good. However, some minor issues still need to be improved: (1) The authors should summarize the main contributions of this paper in Section 1. (2) In Section 4.2, the authors mentioned that “A group will attain a value very close to on GACS if all its accounts have entirely copied their own texts, images or contact information”. However, according to Equation 8, contact information is not considered when computing GACS. (3) In Algorithm 1 on Pg. 17, it seems that “t=t+1” should be added after line 6. (4) I suggest that the limitation of this work should be discussed in Section 9. (5) There are a few typos and grammar errors in this paper.

材料类期刊影响因子

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外文期刊缩写与全称对照表

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SCI英文论文审稿意见汇总

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