Ribocil-C_Racemate_LCMS_27199_MedChemExpress
File ..Data\20171102\20171102-1\BIZ2017-N02-WYQ4.D Tgt Mass (CHM): Injection Date : 2 Nov 17 2:50 pm +0800 Seq. Line : 34 Sample Name : BIZ2017-N02-WYQ4 Location : P1-F-01 Acq. Operator : SYSTEM Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\LCMS03\Data\20171102\20171102-1\1-POS-3MIN.M Analysis Method : D:\LCMS03\Data\20171102\20171102-1\1-POS-3MIN.M Catalog No : HY-19488 Batch#27199
Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min
Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C
min
00.51
1.52
2.5mAU 0
1000
2000
DAD1 A, Sig=214,4 Ref=off 1.1551.178
1.249
1.304
min
00.5
1
1.52
2.5mAU 0
250500
DAD1 B, Sig=254,4 Ref=off 0.463
0.669
01.176
1.2491.3131.357
5981.6
061.730
1.925
2.111
min
00.51 1.52 2.5mV 50
100 ELS1 A, ELSD Signal 1.316
min
00.51 1.52
2.5
2000000
MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70
0.423
1.283
min
0.5
1
1.5
2
2.5
0500000
1000000 Ion 420.1, MSD1 420.1,Target Mass 419.1 +H Positive, EIC=419.8:420.8
1.281
Integration Results for DAD1 A, Sig=214,4 Ref=off
RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.15 0.02 1.67 0.36 0.25 157 1.18 0.01 1.97 0.95 0.30 157 1.25 0.01 660.20 724.10 99.11 420 1.30 0.01 2.29 0.00 0.34 420
Integration Results for DAD1 B, Sig=254,4 Ref=off
RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.46 0.01 0.62 0.94 0.08 157 0.67 0.03 0.59 0.04 0.08 157 1.17 0.02 1.34 1.29 0.17 157 1.18 0.02 3.19 1.19 0.41 157 1.25 0.02 757.75 832.27 98.26 420 1.31 0.02 5.78 4.72 0.75 420 1.36 0.01 0.25 0.44 0.03 420 1.60 0.01 0.27 0.34 0.03 420 1.61 0.02 0.41 0.29 0.05 420 1.73 0.01 0.37 0.51 0.05 420
1.92 0.01 0.27 0.05 0.03 420
2.11 0.01 0.30 0.35 0.04 105 Integration Results for MSD1 TIC, MS File
RetTim Width Area Height Area% MS(+) |-------|--------|--------------|--------------|--------|------|
0.42 0.21 55363972.00 3989297.25 81.08 157
1.28 0.07 12922805.00 2949675.25 18.92 420
Ret. Time: 0.42 <<<< POSITIVE SPECTRA >>>>
m/z
100
200
300
400
500
600
700
800
900
0200000
400000600000800000 ES-API Positive
158.1
157.1
Ret. Time: 1.28
m/z
100
200
300
400
500
600
700
800
900
050000
100000
150000
200000
250000
ES-API Positive
863.3
422.2
421.1
157.1
861.3
420.1
*** End of Report ***